Nonius KappaCCD APEXII diffractometer | 3077 independent reflections |
Radiation source: fine-focus sealed tube | 2864 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.034 |
ω and \ scans | θmax = 67.6°, θmin = 5.1° |
Absorption correction: multi-scan (DENZO; Otwinowski et al., 2003) | h = 0→12 |
Tmin = 0.799, Tmax = 0.944 | k = 0→21 |
8812 measured reflections | l = −13→11 |