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. 2016 Apr 19;72(Pt 5):712–715. doi: 10.1107/S2056989016006058
S1—C1 1.708 (19) C7—C8 1.35 (3)
S1—C3 1.72 (2) C9A—H9AA 0.9700
S2—C1 1.71 (2) C9A—H9AB 0.9700
S2—C2 1.72 (2) C9A—C10A 1.46 (5)
S3—C2 1.72 (2) C9B—H9BA 0.9700
S3—C5A 1.82 (2) C9B—H9BB 0.9700
S3—C5B 1.82 (2) C9B—C10B 1.46 (14)
S4—C3 1.74 (2) C10A—H10A 0.9700
S4—C4 1.82 (2) C10A—H10B 0.9700
S4—C4A 1.82 (2) C10B—H10C 0.9700
S5—C6 1.72 (2) C10B—H10D 0.9700
S5—C7 1.73 (2) Re1—Re2 2.2174 (10)
S6—C6 1.716 (19) Re1—Br1 2.451 (3)
S6—C8 1.72 (2) Re1—Br2 2.451 (2)
S7—C8 1.75 (2) Re1—Br3 2.435 (3)
S7—C9A 1.84 (2) Re1—O2 2.009 (15)
S7—C9B 1.84 (2) Re2—Br4 2.454 (2)
S8—C7 1.75 (2) Re2—Br5 2.465 (2)
S8—C10A 1.84 (2) Re2—Br6 2.473 (2)
S8—C10B 1.84 (2) Re2—O1 2.040 (16)
C1—C6 1.40 (3) O1—C11 1.30 (3)
C2—C3 1.36 (3) O2—C11 1.30 (3)
C4—H4A 0.9700 C11—C12 1.48 (3)
C4—H4B 0.9700 C12—H12A 0.9600
C4—C5B 1.46 (4) C12—H12B 0.9600
C4A—H4AA 0.9700 C12—H12C 0.9600
C4A—H4AB 0.9700 Cl1S—C1S 1.800 (16)
C4A—C5A 1.46 (4) Cl2S—C1S 1.81 (2)
C5A—H5AA 0.9700 Cl2S—H1SA 0.8557
C5A—H5AB 0.9700 C1S—C1Si 1.515 (18)
C5B—H5BA 0.9700 C1S—H1S 0.9700
C5B—H5BB 0.9700 C1S—H1SA 0.9703
C1—S1—C3 94.9 (10) C10A—C9A—H9AA 108.9
C1—S2—C2 95.6 (9) C10A—C9A—H9AB 108.9
C2—S3—C5A 104.3 (14) S7—C9B—H9BA 109.6
C2—S3—C5B 97 (3) S7—C9B—H9BB 109.6
C5A—S3—C5B 19 (3) H9BA—C9B—H9BB 108.1
C3—S4—C4 108 (2) C10B—C9B—S7 110 (7)
C3—S4—C4A 97.4 (15) C10B—C9B—H9BA 109.6
C4A—S4—C4 25 (3) C10B—C9B—H9BB 109.6
C6—S5—C7 94.9 (9) S8—C10A—H10A 109.0
C6—S6—C8 94.9 (10) S8—C10A—H10B 109.0
C8—S7—C9A 98.9 (13) C9A—C10A—S8 113 (2)
C8—S7—C9B 103 (3) C9A—C10A—H10A 109.0
C9A—S7—C9B 26 (4) C9A—C10A—H10B 109.0
C7—S8—C10A 102.8 (12) H10A—C10A—H10B 107.8
C7—S8—C10B 96 (4) S8—C10B—H10C 109.1
C10B—S8—C10A 28 (4) S8—C10B—H10D 109.1
S1—C1—S2 116.1 (11) C9B—C10B—S8 112 (7)
C6—C1—S1 122.7 (15) C9B—C10B—H10C 109.1
C6—C1—S2 121.1 (15) C9B—C10B—H10D 109.1
S3—C2—S2 116.0 (12) H10C—C10B—H10D 107.9
C3—C2—S2 115.7 (15) Re2—Re1—Br1 104.91 (8)
C3—C2—S3 128.3 (16) Re2—Re1—Br2 108.99 (7)
S1—C3—S4 116.6 (12) Re2—Re1—Br3 107.19 (7)
C2—C3—S1 117.5 (15) Br1—Re1—Br2 88.73 (10)
C2—C3—S4 125.9 (17) Br3—Re1—Br1 89.29 (11)
S4—C4—H4A 109.2 Br3—Re1—Br2 143.01 (9)
S4—C4—H4B 109.2 O2—Re1—Re2 91.6 (4)
H4A—C4—H4B 107.9 O2—Re1—Br1 163.4 (4)
C5B—C4—S4 112 (5) O2—Re1—Br2 85.2 (5)
C5B—C4—H4A 109.2 O2—Re1—Br3 86.4 (4)
C5B—C4—H4B 109.2 Re1—Re2—Br4 102.59 (6)
S4—C4A—H4AA 108.8 Re1—Re2—Br5 106.59 (7)
S4—C4A—H4AB 108.8 Re1—Re2—Br6 101.74 (6)
H4AA—C4A—H4AB 107.7 Br4—Re2—Br5 88.72 (9)
C5A—C4A—S4 114 (3) Br4—Re2—Br6 155.47 (8)
C5A—C4A—H4AA 108.8 Br5—Re2—Br6 87.39 (9)
C5A—C4A—H4AB 108.8 O1—Re2—Re1 88.9 (4)
S3—C5A—H5AA 108.1 O1—Re2—Br4 89.9 (5)
S3—C5A—H5AB 108.1 O1—Re2—Br5 164.3 (4)
C4A—C5A—S3 117 (2) O1—Re2—Br6 87.4 (5)
C4A—C5A—H5AA 108.1 C11—O1—Re2 120.9 (14)
C4A—C5A—H5AB 108.1 C11—O2—Re1 119.9 (13)
H5AA—C5A—H5AB 107.3 O1—C11—C12 120 (2)
S3—C5B—H5BA 107.3 O2—C11—O1 118.4 (18)
S3—C5B—H5BB 107.3 O2—C11—C12 121 (2)
C4—C5B—S3 120 (5) C11—C12—H12A 109.5
C4—C5B—H5BA 107.3 C11—C12—H12B 109.5
C4—C5B—H5BB 107.3 C11—C12—H12C 109.5
H5BA—C5B—H5BB 106.9 H12A—C12—H12B 109.5
S6—C6—S5 116.3 (11) H12A—C12—H12C 109.5
C1—C6—S5 122.5 (15) H12B—C12—H12C 109.5
C1—C6—S6 121.2 (15) C1S—Cl2S—H1SA 8.9
S5—C7—S8 114.5 (12) Cl1S—C1S—Cl2S 112 (2)
C8—C7—S5 116.4 (16) Cl1S—C1S—H1S 118.6
C8—C7—S8 129.0 (16) Cl1S—C1S—H1SA 109.2
S6—C8—S7 115.3 (13) Cl2S—C1S—H1S 114.7
C7—C8—S6 117.5 (16) Cl2S—C1S—H1SA 7.8
C7—C8—S7 127.2 (18) C1Si—C1S—Cl1S 97 (2)
S7—C9A—H9AA 108.9 C1Si—C1S—Cl2S 104.2 (12)
S7—C9A—H9AB 108.9 C1Si—C1S—H1S 108.0
H9AA—C9A—H9AB 107.7 C1Si—C1S—H1SA 112.0
C10A—C9A—S7 114 (2) H1S—C1S—H1SA 111.3
S1—C1—C6—S5 0 (3) C7—S8—C10A—C9A 40 (3)
S1—C1—C6—S6 −177.4 (11) C7—S8—C10B—C9B −63 (7)
S2—C1—C6—S5 177.7 (11) C8—S6—C6—S5 0.2 (14)
S2—C1—C6—S6 0 (2) C8—S6—C6—C1 178.1 (17)
S2—C2—C3—S1 2 (3) C8—S7—C9A—C10A 58 (3)
S2—C2—C3—S4 −178.8 (14) C8—S7—C9B—C10B −42 (7)
S3—C2—C3—S1 −177.1 (13) C9A—S7—C8—S6 158.8 (15)
S3—C2—C3—S4 2 (3) C9A—S7—C8—C7 −22 (2)
S4—C4—C5B—S3 58 (9) C9A—S7—C9B—C10B 42 (6)
S4—C4A—C5A—S3 −61 (4) C9B—S7—C8—S6 −175 (4)
S5—C7—C8—S6 1 (2) C9B—S7—C8—C7 4 (4)
S5—C7—C8—S7 −178.2 (13) C9B—S7—C9A—C10A −43 (8)
S7—C9A—C10A—S8 −71 (3) C10A—S8—C7—S5 174.5 (16)
S7—C9B—C10B—S8 77 (9) C10A—S8—C7—C8 −4 (3)
S8—C7—C8—S6 179.3 (13) C10A—S8—C10B—C9B 43 (6)
S8—C7—C8—S7 0 (3) C10B—S8—C7—S5 −158 (4)
C1—S1—C3—S4 176.8 (14) C10B—S8—C7—C8 23 (4)
C1—S1—C3—C2 −4 (2) C10B—S8—C10A—C9A −40 (8)
C1—S2—C2—S3 −179.7 (12) Re1—Re2—O1—C11 −3.2 (15)
C1—S2—C2—C3 0.9 (19) Re1—O2—C11—O1 −6 (2)
C2—S2—C1—S1 −3.7 (13) Re1—O2—C11—C12 175.2 (17)
C2—S2—C1—C6 178.7 (17) Re2—Re1—O2—C11 3.0 (15)
C2—S3—C5A—C4A 22 (4) Re2—O1—C11—O2 6 (3)
C2—S3—C5B—C4 −61 (7) Re2—O1—C11—C12 −175.0 (17)
C3—S1—C1—S2 4.6 (14) Br1—Re1—Re2—Br4 −90.90 (10)
C3—S1—C1—C6 −177.8 (18) Br1—Re1—Re2—Br5 1.54 (11)
C3—S4—C4—C5B −19 (7) Br1—Re1—Re2—Br6 92.30 (10)
C3—S4—C4A—C5A 63 (3) Br1—Re1—Re2—O1 179.4 (5)
C4—S4—C3—S1 168 (3) Br1—Re1—O2—C11 −174.7 (11)
C4—S4—C3—C2 −11 (4) Br2—Re1—Re2—Br4 175.23 (10)
C4—S4—C4A—C5A −54 (6) Br2—Re1—Re2—Br5 −92.32 (10)
C4A—S4—C3—S1 144.9 (18) Br2—Re1—Re2—Br6 −1.56 (10)
C4A—S4—C3—C2 −34 (3) Br2—Re1—Re2—O1 85.6 (5)
C4A—S4—C4—C5B 50 (4) Br2—Re1—O2—C11 −105.9 (15)
C5A—S3—C2—S2 −169.7 (19) Br3—Re1—Re2—Br4 3.05 (11)
C5A—S3—C2—C3 10 (3) Br3—Re1—Re2—Br5 95.49 (11)
C5A—S3—C5B—C4 53 (6) Br3—Re1—Re2—Br6 −173.75 (10)
C5B—S3—C2—S2 −152 (3) Br3—Re1—Re2—O1 −86.6 (5)
C5B—S3—C2—C3 28 (3) Br3—Re1—O2—C11 110.1 (15)
C5B—S3—C5A—C4A −48 (8) Br4—Re2—O1—C11 −105.8 (15)
C6—S5—C7—S8 −179.3 (12) Br5—Re2—O1—C11 169.2 (11)
C6—S5—C7—C8 −0.5 (19) Br6—Re2—O1—C11 98.6 (15)
C6—S6—C8—S7 178.5 (13) O2—Re1—Re2—Br4 89.8 (5)
C6—S6—C8—C7 −0.6 (19) O2—Re1—Re2—Br5 −177.8 (5)
C7—S5—C6—S6 0.1 (14) O2—Re1—Re2—Br6 −87.0 (5)
C7—S5—C6—C1 −177.7 (18) O2—Re1—Re2—O1 0.1 (6)