| Crystal data |
| Chemical formula |
(C10H8S8)[Re2Br6(C2H3O2)]·0.5C2H3Cl3
|
|
M
r
|
1362.24 |
| Crystal system, space group |
Monoclinic, I2/a
|
| Temperature (K) |
298 |
|
a, b, c (Å) |
27.1825 (5), 8.53737 (13), 26.0667 (5) |
| β (°) |
100.8440 (17) |
|
V (Å3) |
5941.21 (18) |
|
Z
|
8 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
16.93 |
| Crystal size (mm) |
0.4 × 0.4 × 0.1 |
| |
| Data collection |
| Diffractometer |
Agilent Xcalibur Sapphire3 |
| Absorption correction |
Multi-scan (CrysAlis PRO; Agilent, 2014 ▸) |
|
T
min, T
max
|
0.067, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
36051, 6755, 6304 |
|
R
int
|
0.039 |
| (sin θ/λ)max (Å−1) |
0.650 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.052, 0.137, 1.14 |
| No. of reflections |
6755 |
| No. of parameters |
334 |
| No. of restraints |
99 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
1.77, −1.90 |
