Table 2. Experimental details.
| Crystal data | |
| Chemical formula | [Ni(C7H3NO4)(C4H4N2)(C2H6OS)] |
| M r | 382.03 |
| Crystal system, space group | Monoclinic, P21/m |
| Temperature (K) | 100 |
| a, b, c (Å) | 10.5631 (7), 7.0296 (4), 20.3710 (13) |
| β (°) | 90.6447 (11) |
| V (Å3) | 1512.54 (16) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 1.45 |
| Crystal size (mm) | 0.37 × 0.15 × 0.05 |
| Data collection | |
| Diffractometer | Bruker APEXII DUO CCD |
| Absorption correction | Analytical based on measured indexed crystal faces; XPREP (Bruker, 2014 ▸) |
| T min, T max | 0.730, 0.965 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 56634, 3756, 3549 |
| R int | 0.026 |
| (sin θ/λ)max (Å−1) | 0.650 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.020, 0.055, 1.07 |
| No. of reflections | 3756 |
| No. of parameters | 256 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.43, −0.31 |