| Crystal data |
| Chemical formula |
(C10H28N4)[Cr2O7]2
|
|
M
r
|
636.36 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
293 |
|
a, b, c (Å) |
8.5361 (3), 8.6272 (3), 8.8576 (3) |
| α, β, γ (°) |
77.761 (1), 72.307 (1), 60.985 (1) |
|
V (Å3) |
541.81 (3) |
|
Z
|
1 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
2.03 |
| Crystal size (mm) |
0.35 × 0.30 × 0.25 |
| |
| Data collection |
| Diffractometer |
Bruker Kappa APEXII CCD |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2004 ▸) |
|
T
min, T
max
|
0.528, 0.649 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
10263, 1913, 1835 |
|
R
int
|
0.020 |
| (sin θ/λ)max (Å−1) |
0.595 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.023, 0.068, 1.06 |
| No. of reflections |
1913 |
| No. of parameters |
145 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.44, −0.45 |
