| Crystal data |
| Chemical formula |
C23H14ClFO |
|
M
r
|
360.79 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
296 |
|
a, b, c (Å) |
9.2846 (9), 9.8777 (10), 10.3624 (11) |
| α, β, γ (°) |
94.364 (2), 113.3517 (19), 92.866 (2) |
|
V (Å3) |
866.63 (15) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.24 |
| Crystal size (mm) |
0.43 × 0.39 × 0.11 |
| |
| Data collection |
| Diffractometer |
Bruker SMART APEXII DUO CCD |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2009 ▸) |
|
T
min, T
max
|
0.905, 0.974 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
15408, 3917, 2973 |
|
R
int
|
0.027 |
| (sin θ/λ)max (Å−1) |
0.650 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.046, 0.159, 1.04 |
| No. of reflections |
3917 |
| No. of parameters |
235 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) |
0.27, −0.38 |
