| Rigaku Saturn944+ diffractometer | 3706 independent reflections |
| Radiation source: Sealed Tube | 3362 reflections with I > 2σ(I) |
| Confocal monochromator | Rint = 0.037 |
| Detector resolution: 22.2222 pixels mm-1 | θmax = 68.2°, θmin = 3.7° |
| profile data from ω–scans | h = −29→28 |
| Absorption correction: multi-scan (CrystalClear-SM Expert; Rigaku, 2012) | k = −10→10 |
| Tmin = 0.814, Tmax = 1.000 | l = −8→11 |
| 18993 measured reflections |
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