Oxford Diffraction Xcalibur 3/Sapphire3 CCD diffractometer	2668 independent reflections
Radiation source: Enhance (Mo) X-ray Source	2637 reflections with I > 2σ(I)
Graphite monochromator	Rint = 0.031
Detector resolution: 16.0050 pixels mm-1	θmax = 30.0°, θmin = 3.8°
Thin–slice φ and ω scans	h = −6→6
Absorption correction: multi-scan (CrysAlis PRO; Agilent, 2014)	k = −8→8
Tmin = 0.608, Tmax = 1.000	l = −12→12
4256 measured reflections