| Crystal data |
| Chemical formula |
(CH6N3)[Mn(C2O4)Cl(H2O)]·H2O |
|
M
r
|
274.53 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
298 |
|
a, b, c (Å) |
6.740 (5), 7.514 (7), 9.810 (2) |
| α, β, γ (°) |
84.46 (3), 78.15 (4), 88.57 (6) |
|
V (Å3) |
484.0 (6) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
1.65 |
| Crystal size (mm) |
0.50 × 0.43 × 0.34 |
| |
| Data collection |
| Diffractometer |
Enraf–Nonius CAD-4 |
| Absorption correction |
ψ scan (North et al., 1968 ▸) |
|
T
min, T
max
|
0.551, 0.718 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
4226, 2114, 2018 |
|
R
int
|
0.016 |
| (sin θ/λ)max (Å−1) |
0.638 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.024, 0.065, 1.10 |
| No. of reflections |
2114 |
| No. of parameters |
155 |
| No. of restraints |
11 |
| H-atom treatment |
H-atom parameters not refined |
| Δρmax, Δρmin (e Å−3) |
0.39, −0.30 |
