| Crystal data |
| Chemical formula |
[Co2Na2O(C6H18NSi2)4] |
|
M
r
|
821.41 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
100 |
|
a, b, c (Å) |
8.8839 (18), 10.591 (2), 12.700 (3) |
| α, β, γ (°) |
96.75 (4), 108.93 (3), 99.15 (3) |
|
V (Å3) |
1097.4 (5) |
|
Z
|
1 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
1.02 |
| Crystal size (mm) |
0.30 × 0.24 × 0.20 |
| |
| Data collection |
| Diffractometer |
Bruker SMART
APEX CCD |
| Absorption correction |
Multi-scan (TWINABS; Bruker,2012 ▸) |
|
T
min, T
max
|
0.57, 0.75 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
4421, 4421, 3107 |
|
R
int
|
0.089 |
| (sin θ/λ)max (Å−1) |
0.627 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.065, 0.154, 1.03 |
| No. of reflections |
4421 |
| No. of parameters |
200 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
1.08, −0.54 |
