| Crystal data |
| Chemical formula |
[Mn(C4H11NO2)2](C7H6NO2)2
|
|
M
r
|
537.47 |
| Crystal system, space group |
Orthorhombic, P
b
c
a
|
| Temperature (K) |
293 |
|
a, b, c (Å) |
10.6120 (4), 10.8219 (4), 21.7591 (8) |
|
V (Å3) |
2498.86 (15) |
|
Z
|
4 |
| Radiation type |
Cu Kα |
| μ (mm−1) |
4.76 |
| Crystal size (mm) |
0.32 × 0.20 × 0.18 |
| |
| Data collection |
| Diffractometer |
Oxford Diffraction Xcalibur Ruby |
| Absorption correction |
Multi-scan (CrysAlis PRO; Oxford Diffraction, 2009 ▸) |
|
T
min, T
max
|
0.932, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
10631, 2589, 1740 |
|
R
int
|
0.056 |
| (sin θ/λ)max (Å−1) |
0.630 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.045, 0.136, 1.06 |
| No. of reflections |
2589 |
| No. of parameters |
180 |
| No. of restraints |
3 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) |
0.37, −0.22 |
