Bruker APEXII diffractometer | 3031 independent reflections |
Radiation source: fine-focus sealed tube | 2930 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.040 |
phi and φ scans | θmax = 64.4°, θmin = 3.3° |
Absorption correction: multi-scan (SADABS; Bruker, 2009) | h = −8→8 |
Tmin = 0.245, Tmax = 0.278 | k = −11→11 |
11112 measured reflections | l = −15→16 |