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. 2016 Mar 11;72(Pt 4):477–481. doi: 10.1107/S2056989016003777
Br1B—C1B 1.897 (3) C2A—C1A 1.391 (5)
Br1A—C1A 1.901 (3) C5A—C6A 1.387 (5)
O3B—C2B 1.371 (4) C5A—H5A 0.9500
O3B—C8B 1.428 (4) C3A—H3A 0.9500
O3A—C2A 1.374 (4) C3B—C2B 1.385 (5)
O3A—C8A 1.430 (4) C3B—H3B 0.9500
O4B—C8B 1.390 (4) C2B—C1B 1.400 (5)
O4B—C9B 1.426 (4) C5B—C6B 1.373 (5)
O4A—C8A 1.383 (4) C5B—H5B 0.9500
O4A—C9A 1.426 (4) C6B—C1B 1.380 (5)
O1A—C7A 1.260 (4) C6B—H6B 0.9500
O2A—C7A 1.279 (4) C6A—C1A 1.383 (5)
O2A—H2A 0.83 (3) C6A—H6A 0.9500
O1B—C7B 1.275 (4) C9A—H9A1 0.9800
O2B—C7B 1.271 (4) C9A—H9A2 0.9800
O2B—H2B 0.82 (3) C9A—H9A3 0.9800
C4A—C5A 1.395 (5) C8A—H8A1 0.9900
C4A—C3A 1.398 (4) C8A—H8A2 0.9900
C4A—C7A 1.482 (5) C8B—H8B1 0.9900
C7B—C4B 1.476 (5) C8B—H8B2 0.9900
C4B—C5B 1.394 (5) C9B—H9B1 0.9800
C4B—C3B 1.402 (4) C9B—H9B2 0.9800
C2A—C3A 1.386 (5) C9B—H9B3 0.9800
C2B—O3B—C8B 117.7 (2) C5B—C6B—C1B 120.4 (3)
C2A—O3A—C8A 118.1 (2) C5B—C6B—H6B 119.8
C8B—O4B—C9B 113.7 (3) C1B—C6B—H6B 119.8
C8A—O4A—C9A 113.3 (3) C6B—C1B—C2B 121.2 (3)
C7A—O2A—H2A 116 (3) C6B—C1B—Br1B 118.9 (3)
C7B—O2B—H2B 124 (4) C2B—C1B—Br1B 119.9 (2)
C5A—C4A—C3A 120.9 (3) C1A—C6A—C5A 119.5 (3)
C5A—C4A—C7A 120.5 (3) C1A—C6A—H6A 120.2
C3A—C4A—C7A 118.5 (3) C5A—C6A—H6A 120.2
O2B—C7B—O1B 123.3 (3) O4A—C9A—H9A1 109.5
O2B—C7B—C4B 117.5 (3) O4A—C9A—H9A2 109.5
O1B—C7B—C4B 119.1 (3) H9A1—C9A—H9A2 109.5
C5B—C4B—C3B 120.6 (3) O4A—C9A—H9A3 109.5
C5B—C4B—C7B 119.9 (3) H9A1—C9A—H9A3 109.5
C3B—C4B—C7B 119.4 (3) H9A2—C9A—H9A3 109.5
O3A—C2A—C3A 124.7 (3) O4A—C8A—O3A 113.1 (3)
O3A—C2A—C1A 116.6 (3) O4A—C8A—H8A1 109.0
C3A—C2A—C1A 118.6 (3) O3A—C8A—H8A1 109.0
O1A—C7A—O2A 123.3 (3) O4A—C8A—H8A2 109.0
O1A—C7A—C4A 118.9 (3) O3A—C8A—H8A2 109.0
O2A—C7A—C4A 117.8 (3) H8A1—C8A—H8A2 107.8
C6A—C5A—C4A 119.2 (3) O4B—C8B—O3B 113.0 (3)
C6A—C5A—H5A 120.4 O4B—C8B—H8B1 109.0
C4A—C5A—H5A 120.4 O3B—C8B—H8B1 109.0
C2A—C3A—C4A 119.8 (3) O4B—C8B—H8B2 109.0
C2A—C3A—H3A 120.1 O3B—C8B—H8B2 109.0
C4A—C3A—H3A 120.1 H8B1—C8B—H8B2 107.8
C2B—C3B—C4B 119.7 (3) C6A—C1A—C2A 122.0 (3)
C2B—C3B—H3B 120.1 C6A—C1A—Br1A 119.1 (3)
C4B—C3B—H3B 120.1 C2A—C1A—Br1A 119.0 (2)
O3B—C2B—C3B 124.8 (3) O4B—C9B—H9B1 109.5
O3B—C2B—C1B 116.4 (3) O4B—C9B—H9B2 109.5
C3B—C2B—C1B 118.8 (3) H9B1—C9B—H9B2 109.5
C6B—C5B—C4B 119.3 (3) O4B—C9B—H9B3 109.5
C6B—C5B—H5B 120.4 H9B1—C9B—H9B3 109.5
C4B—C5B—H5B 120.4 H9B2—C9B—H9B3 109.5
O2B—C7B—C4B—C5B −8.5 (4) C4B—C3B—C2B—C1B 0.0 (4)
O1B—C7B—C4B—C5B 170.4 (3) C3B—C4B—C5B—C6B 1.7 (4)
O2B—C7B—C4B—C3B 172.9 (3) C7B—C4B—C5B—C6B −176.9 (3)
O1B—C7B—C4B—C3B −8.3 (4) C4B—C5B—C6B—C1B −0.6 (4)
C8A—O3A—C2A—C3A 2.2 (4) C5B—C6B—C1B—C2B −0.8 (4)
C8A—O3A—C2A—C1A −178.5 (3) C5B—C6B—C1B—Br1B 176.5 (2)
C5A—C4A—C7A—O1A −175.6 (3) O3B—C2B—C1B—C6B 180.0 (3)
C3A—C4A—C7A—O1A 0.8 (4) C3B—C2B—C1B—C6B 1.1 (4)
C5A—C4A—C7A—O2A 2.4 (4) O3B—C2B—C1B—Br1B 2.7 (4)
C3A—C4A—C7A—O2A 178.9 (3) C3B—C2B—C1B—Br1B −176.2 (2)
C3A—C4A—C5A—C6A −1.5 (4) C4A—C5A—C6A—C1A −0.4 (4)
C7A—C4A—C5A—C6A 174.8 (3) C9A—O4A—C8A—O3A −65.8 (3)
O3A—C2A—C3A—C4A −180.0 (3) C2A—O3A—C8A—O4A −65.6 (3)
C1A—C2A—C3A—C4A 0.7 (4) C9B—O4B—C8B—O3B −74.1 (3)
C5A—C4A—C3A—C2A 1.3 (4) C2B—O3B—C8B—O4B −76.2 (3)
C7A—C4A—C3A—C2A −175.1 (3) C5A—C6A—C1A—C2A 2.5 (4)
C5B—C4B—C3B—C2B −1.4 (4) C5A—C6A—C1A—Br1A −177.4 (2)
C7B—C4B—C3B—C2B 177.2 (3) O3A—C2A—C1A—C6A 178.0 (3)
C8B—O3B—C2B—C3B 7.7 (4) C3A—C2A—C1A—C6A −2.6 (4)
C8B—O3B—C2B—C1B −171.1 (3) O3A—C2A—C1A—Br1A −2.2 (4)
C4B—C3B—C2B—O3B −178.8 (3) C3A—C2A—C1A—Br1A 177.2 (2)