| Crystal data |
| Chemical formula |
[PdCl2(C11H9N)(C13H14N2)] |
|
M
r
|
530.75 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
183 |
|
a, b, c (Å) |
7.8768 (3), 12.2939 (5), 12.6120 (4) |
| α, β, γ (°) |
95.692 (3), 97.267 (3), 103.574 (3) |
|
V (Å3) |
1167.09 (8) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
1.04 |
| Crystal size (mm) |
0.39 × 0.27 × 0.1 |
| |
| Data collection |
| Diffractometer |
Agilent Xcalibur Ruby |
| Absorption correction |
Analytical (CrysAlis PRO; Agilent, 2012 ▸) |
|
T
min, T
max
|
0.727, 0.916 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
28730, 7116, 6179 |
|
R
int
|
0.037 |
| (sin θ/λ)max (Å−1) |
0.714 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.027, 0.068, 1.04 |
| No. of reflections |
7116 |
| No. of parameters |
272 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.45, −0.42 |
