| Bruker APEXII diffractometer | 1796 reflections with I > 2σ(I) |
| Radiation source: fine-focus sealed tube | Rint = 0.056 |
| Graphite monochromator | θmax = 64.1°, θmin = 5.1° |
| phi and φ scans | h = −10→10 |
| Absorption correction: multi-scan (SADABS; Bruker, 2009) | k = −14→14 |
| Tmin = 0.557, Tmax = 0.649 | l = −10→13 |
| 8422 measured reflections | 1 standard reflections every 1 reflections |
| 2115 independent reflections | intensity decay: 0.1% |