| Crystal data |
| Chemical formula |
[Cu(C7H3NO4)(C5H6N2)(C3H7NO)] |
|
M
r
|
395.86 |
| Crystal system, space group |
Orthorhombic, P212121
|
| Temperature (K) |
293 |
|
a, b, c (Å) |
8.3365 (17), 10.453 (2), 19.030 (4) |
|
V (Å3) |
1658.2 (6) |
|
Z
|
4 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
1.35 |
| Crystal size (mm) |
0.24 × 0.20 × 0.19 |
| |
| Data collection |
| Diffractometer |
Bruker APEXII DUO CCD |
| Absorption correction |
Analytical [based on measured indexed crystal faces using SHELXL2014 (Sheldrick, 2015b
▸)] |
|
T
min, T
max
|
0.716, 0.773 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
16376, 3799, 2926 |
|
R
int
|
0.051 |
| (sin θ/λ)max (Å−1) |
0.649 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.039, 0.132, 1.15 |
| No. of reflections |
3799 |
| No. of parameters |
226 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.79, −1.17 |
| Absolute structure |
Flack (1983 ▸), 1619 Friedel pairs |
| Absolute structure parameter |
0.00 (2) |
