Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C15H24O2 |
| M r | 236.34 |
| Crystal system, space group | Monoclinic, P21 |
| Temperature (K) | 299 |
| a, b, c (Å) | 8.849 (4), 5.336 (1), 14.994 (5) |
| β (°) | 99.21 (2) |
| V (Å3) | 698.9 (4) |
| Z | 2 |
| Radiation type | Cu Kα |
| μ (mm−1) | 0.56 |
| Crystal size (mm) | 0.50 × 0.18 × 0.15 |
| Data collection | |
| Diffractometer | Enraf–Nonius CAD-4 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 1916, 1392, 1260 |
| R int | 0.052 |
| (sin θ/λ)max (Å−1) | 0.597 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.060, 0.164, 1.10 |
| No. of reflections | 1392 |
| No. of parameters | 154 |
| No. of restraints | 1 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.46, −0.22 |