| Crystal data |
| Chemical formula |
[Eu(C3H7NO)8][PMo12O40] |
|
M
r
|
2558.97 |
| Crystal system, space group |
Orthorhombic, P
n
a21
|
| Temperature (K) |
296 |
|
a, b, c (Å) |
26.9108 (10), 18.3506 (6), 13.4494 (4) |
|
V (Å3) |
6641.7 (4) |
|
Z
|
4 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
3.24 |
| Crystal size (mm) |
0.20 × 0.18 × 0.17 |
| |
| Data collection |
| Diffractometer |
Bruker APEXII CCD |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2006 ▸) |
|
T
min, T
max
|
0.667, 0.747 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
88354, 33285, 19583 |
|
R
int
|
0.075 |
| (sin θ/λ)max (Å−1) |
0.849 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.047, 0.095, 0.98 |
| No. of reflections |
33285 |
| No. of parameters |
863 |
| No. of restraints |
1 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
2.08, −1.80 |
| Absolute structure |
Flack x determined using 6924 quotients [(I
+)−(I
−)]/[(I
+)+(I
−)] |
| Absolute structure parameter |
−0.015 (7) |
