| Crystal data |
| Chemical formula |
[Cr2Pb2(NCS)2(OH)2(C4H10NO)4](NCS)2·C2H3N |
|
M
r
|
1178.29 |
| Crystal system, space group |
Monoclinic, C2/c
|
| Temperature (K) |
298 |
|
a, b, c (Å) |
17.533 (1), 13.8815 (7), 16.6179 (8) |
| β (°) |
104.771 (6) |
|
V (Å3) |
3910.9 (4) |
|
Z
|
4 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
9.39 |
| Crystal size (mm) |
0.4 × 0.1 × 0.1 |
| |
| Data collection |
| Diffractometer |
Agilent Xcalibur Sapphire 3 |
| Absorption correction |
Multi-scan (CrysAlis PRO; Agilent, 2011 ▸) |
|
T
min, T
max
|
0.382, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
20193, 5680, 4133 |
|
R
int
|
0.064 |
| (sin θ/λ)max (Å−1) |
0.703 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.035, 0.058, 0.93 |
| No. of reflections |
5680 |
| No. of parameters |
190 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
1.00, −0.69 |
