Table 5. Experimental details.
| Crystal data | |
| Chemical formula | C16H16N2O2S2 |
| M r | 332.43 |
| Crystal system, space group | Monoclinic, C2/c |
| Temperature (K) | 100 |
| a, b, c (Å) | 20.7896 (10), 4.6965 (2), 32.5217 (13) |
| β (°) | 95.004 (4) |
| V (Å3) | 3163.3 (2) |
| Z | 8 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.35 |
| Crystal size (mm) | 0.25 × 0.15 × 0.07 |
| Data collection | |
| Diffractometer | Agilent Xcalibur Eos Gemini |
| Absorption correction | Multi-scan (CrysAlis PRO; Agilent, 2011 ▸) |
| T min, T max | 0.87, 0.98 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 6979, 3270, 2595 |
| R int | 0.033 |
| (sin θ/λ)max (Å−1) | 0.628 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.041, 0.097, 1.06 |
| No. of reflections | 3270 |
| No. of parameters | 206 |
| No. of restraints | 2 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) | 0.33, −0.24 |