Table 3. Experimental details.
| Crystal data | |
| Chemical formula | [Co(C10H11O2)2(C10H14N2O)2(H2O)2] |
| M r | 777.80 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 100 |
| a, b, c (Å) | 12.9646 (4), 10.8636 (3), 15.6297 (5) |
| β (°) | 111.596 (3) |
| V (Å3) | 2046.79 (12) |
| Z | 2 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.47 |
| Crystal size (mm) | 0.45 × 0.40 × 0.33 |
| Data collection | |
| Diffractometer | Bruker SMART BREEZE CCD |
| Absorption correction | Multi-scan (SADABS; Bruker, 2012 ▸) |
| T min, T max | 0.754, 0.861 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 42492, 5124, 3701 |
| R int | 0.041 |
| (sin θ/λ)max (Å−1) | 0.670 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.063, 0.155, 1.07 |
| No. of reflections | 5124 |
| No. of parameters | 270 |
| No. of restraints | 42 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) | 0.63, −0.39 |