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. 2016 Mar 31;72(Pt 4):556–558. doi: 10.1107/S2056989016004497

Table 2. Experimental details.

Crystal data
Chemical formula C8H8N6
M r 188.20
Crystal system, space group Monoclinic, P21/n
Temperature (K) 150
a, b, c (Å) 5.0618 (3), 14.6282 (8), 6.1294 (4)
β (°) 106.321 (2)
V3) 435.56 (5)
Z 2
Radiation type Mo Kα
μ (mm−1) 0.10
Crystal size (mm) 0.35 × 0.10 × 0.03
 
Data collection
Diffractometer Bruker D8 VENTURE
Absorption correction Multi-scan (SADABS; Bruker, 2015)
T min, T max 0.702, 0.746
No. of measured, independent and observed [I > 2σ(I)] reflections 2614, 999, 903
R int 0.014
(sin θ/λ)max−1) 0.650
 
Refinement
R[F 2 > 2σ(F 2)], wR(F 2), S 0.042, 0.117, 1.12
No. of reflections 999
No. of parameters 68
H-atom treatment H atoms treated by a mixture of independent and constrained refinement
Δρmax, Δρmin (e Å−3) 0.31, −0.26

Computer programs: APEX3 and SAINT (Bruker, 2015), SHELXS97 and SHELXTL (Sheldrick, 2008) and SHELXL2014 (Sheldrick, 2015).