| Crystal data |
| Chemical formula |
(C11H17N2)[ZrCl6]·2CH2Cl2
|
|
M
r
|
828.30 |
| Crystal system, space group |
Monoclinic, P21/n
|
| Temperature (K) |
200 |
|
a, b, c (Å) |
10.443 (5), 16.154 (9), 10.891 (6) |
| β (°) |
91.259 (10) |
|
V (Å3) |
1836.9 (17) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
1.05 |
| Crystal size (mm) |
0.20 × 0.20 × 0.15 |
| |
| Data collection |
| Diffractometer |
Bruker SMART area-detector |
| Absorption correction |
Multi-scan (SADABS; Sheldrick, 1996 ▸) |
|
T
min, T
max
|
0.818, 0.859 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
10309, 3410, 2255 |
|
R
int
|
0.061 |
| (sin θ/λ)max (Å−1) |
0.606 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.071, 0.213, 1.00 |
| No. of reflections |
3410 |
| No. of parameters |
181 |
| No. of restraints |
1 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
1.73, −0.90 |
