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. Author manuscript; available in PMC: 2017 Feb 8.
Published in final edited form as: ACS Biomater Sci Eng. 2016 Jan 6;2(2):268–277. doi: 10.1021/acsbiomaterials.5b00534

Table 1.

Optimization of Polymerization and atRA Incorporation Conditionsa

conditions atRA
recrystallization
polymerization
time
atRA structure
retention
60 °C,
  10% w/w
yes 5 days nt
37 °C,
  10% w/w
yes 20 days nt
60 °C,
  30% w/w
no 5 days yes
37 °C,
  30% w/w
no 20 days no
a

nt: not tested.

atRA concentration was 4 mg/mL. Structure retention assessed using HPLC. x% w/w indicates POC concentration in ethanol used.