Table 1.
conditions | atRA recrystallization |
polymerization time |
atRA structure retention |
---|---|---|---|
60 °C, 10% w/w |
yes | 5 days | nt |
37 °C, 10% w/w |
yes | 20 days | nt |
60 °C, 30% w/w |
no | 5 days | yes |
37 °C, 30% w/w |
no | 20 days | no |
nt: not tested.
atRA concentration was 4 mg/mL. Structure retention assessed using HPLC. x% w/w indicates POC concentration in ethanol used.