Table 5.

¹H and ¹³C NMR spectral data for compounds 3, 4, and 5

Position	3		4		5
	δH	δC	δH	δC	δH	δC
2	6.9, br d	133.6, d	7.2, d(7.6)	130.1, d	6.9, d(6.8)	133.2, d
3	6.8, br d	100.9, d	6.4, d(7.2)	101.5, d	6.8, br d	113.3, d
3a		148.9, s		151.9, s		146.1, s
5	7.5, br d	147.2, d	7.9, d(7.2)	148.1, d	7.5, d(6.4)	146.1, d
6	7.3, br d	113.5, d	7.7, d(7.2)	113.6, d	7.5, d(6.4)	116.4, d
6a		136.3, s		136.4, s		136.6, s
7	6.8, br s	100.3, d	7.0, s	98.8, d	6.8, s	99.9, d
8		157.2, s		157.9, s		156.7, s
9		126.9, s		124.4, s		134.7, s
9a		124.0, s		127.3, s		124.3, s
9b		117.8, s		117.6, s		117.9, s
NCH3	3.8, s	45.4, q	4.0, s	44.8, q	3.9, s	45.0, q
OCH3	3.9, s	56.8, q	3.9, s	56.2, q	3.9, s	56.6, q
1′		165.4, s		164.9, s		164.0, s
2′		134.9, s		125.6, s		123.3, s
3′		141.9, s	8.1, d(8)	130.4, d	8.2, br d	133.1, d
4′	7.1, br d	130.9, d	7.46, d(8)	128.3, d	7.2, br d	114.5, d
5′	7.5, br d	132.2, d		149.1, s		167.8, s
6′	7.3, br d	126.3, d	7.46, d(8)	128.3, d	7.2, br d	114.5, d
7′	8.1, d(7.6)	131.5, d	8.1, d(8)	130.4, d	8.2, br d	133.1, d
8′	2.6, s	21.8, q	2.7, q(7.6)	28.6, t		F
9′			1.3, t(7.6)	14.3, t

Measured in CDCl₃ at 400 MHz for ¹H and 100 MHz for ¹³C, respectively. J values in Hz.