Table 8.

¹H and ¹³C NMR spectral data for compounds 12, 13, and 14

Position	12		13		14
	δH	δC	δH	δC	δH	δC
2	7.2, br d	119.8, d	7.0, d(5.6)	127.8, d	7.0, d(7.2)	131.8, d
3	6.8, br d	100.6, d	6.8, d(5.6)	103.5, d	6.8, br d	113.4, d
3a		136.6, s		150.8, s		150.3, s
5	7.5, br d	131.6, d	8.0, br d	144.4, d	7.5, d(6.8)	147.1, d
6	7.5, br d	113.5, d	7.2, d(6.8)	113.4, d	7.4, br d	127.8, d
6a		126.3, s		136.8, s		136.1, s
7	6.8, s	100.6, d	6.6, s	98.6, d	6.8, s	100.7, d
8		153.7, s		156.2, s		156.9, s
9		134.9, s		134.9, s		134.5, s
9a		118.9, s		123.0, s		123.6, s
9b		117.9, s		118.8, s		117.5, s
NCH3	3.9, s	45.5, q	3.7, s	44.7, q	3.9, s	45.3, q
OCH3	3.9, s	56.8, q	3.8, s	56.4, q	3.9, s	56.8, q
1′		157.1, s		165.2, s		164.9, s
2′		123.7, s		125.8, s		125.4, s
3′	8.2, d(6.8)	132.7, d	8.1, d(8)	130.6, d	8.1, d(7.6)	130.6, d
4′	7.4, d(7.2)	120.7, d	7.3, d(8)	129.0, d	7.3, br d	129.0, d
5′		163.8, s		150.1, s		148.9, s
6′	7.4, d(7.2)	120.7, d	7.3, d(8)	129.0, d	7.3, br d	129.0, d
7′	8.2, d(6.8)	132.7, d	8.1, d(8)	130.6, d	8.1, d(7.6)	130.6, d
8′			2.7, t(7.6)	35.8, t	2.7, t(8)	36.0, t
9′			1.6, m(7.6)	33.2, t	1.7, br m	31.4, t
10′			1.4, m(7.6)	22.3, t	1.3, br m	30.7, t
11′			0.9, t(7.6)	13.9, q	1.3, br m	22.4, t
12′					0.9, br t	13.9, t

Measured in CDCl₃ at 400 MHz for ¹H and 100 MHz for ¹³C, respectively. J values in Hz.