Table 2. Data collection and processing for the acetate-free CueO crystal.
Values in parentheses are for the outer shell.
| Diffraction source | BL26B2, SPring-8 |
| Wavelength (Å) | 0.8000 |
| Temperature (K) | 100 |
| Detector | MAR Research MX225 |
| Crystal-to-detector distance (mm) | 200.0 |
| Rotation range per image (°) | 1 |
| Total rotation range (°) | 180 |
| Exposure time per image (s) | 1 |
| Attenuator | Al, 1000 µm |
| Space group | P21 |
| a, b, c (Å) | 50.28, 93.24, 59.59 |
| α, β, γ (°) | 90.00, 112.87, 90.00 |
| Resolution range (Å) | 17.60–1.90 (1.97–19.0) |
| No. of unique reflections | 38421 (3579) |
| Completeness (%) | 98.7 (92.1) |
| Multiplicity | 3.7 (2.9) |
| 〈I/σ(I)〉 | 10.4 (2.0) |
| R r.i.m. † | 0.094 (0.343) |
| R | 0.154 (0.213) |
| R free | 0.184 (0.254) |
†
R r.i.m. was estimated by multiplying the conventional R merge value by the factor [N/(N − 1)]1/2, where N is the data multiplicity.