TABLE 1.
Data and refinement statistics
| Data collection statistics for APS-SBC-19ID | |
| Space group | P212121 |
| Unit cell (Å) | |
| a | 116.4 |
| b | 124.3 |
| c | 180.0 |
| Resolution (Å) | 38.2–1.93 |
| Wavelength (Å) | 0.9794 |
| No. of observed reflections | 204,709 |
| No. of unique reflections | 48,738 |
| Rpima (%) | 4.0 (61.1)b |
| Completeness (%) | 97.7 (96.8) |
| I/δ | 19.1 (1.5) |
| Phasing | |
| Phasing method | SADc |
| Refinement statistics | |
| Rcryst (%) | 13.90 |
| Rfree (%) | 16.94 |
| Protein residues | 1866 |
| Sodium/phosphate/glycerol/acetate molecules | 2/4/2/2 |
| Solvent | 2185 |
| Root mean square deviation from target values | |
| Bond lengths (Å) | 0.011 |
| Bond angles (degrees) | 1.22 |
| Average B factors (Å2) | |
| Protein | 27.8 |
| Ions | 46.0 |
| Solvent | 37.8 |
| PDB code | 4ZMH |
| Ramachandran (%) F/A/Od | 97/3.0/0 |
a Rpim = Σhkl(1/(N − 1)½)Σi|Ii(hkl) − Īhkl|/ΣhklΣiIi(hkl).
b Numbers in parentheses are values for the highest resolution bin.
c Single-wavelength anomalous diffraction.
d As defined by MOLPROBITY (F (favored)/A (allowed)/O (outliers)).