Table 1. Crystallographic data collection and refinement statistics.
| NP-nucleozin(PDB code 4 × 9A) | |
|---|---|
| Data collection | |
| Space group | C2 |
| Cell dimensions | |
| a, b, c (Å) | 129.0, 121.6, 195.5 |
| α, β, γ (°) | 90.00, 89.79, 90.00 |
| Resolution (Å) | 50~3.00(3.11~3.00) |
| Unique reflections | 55770(5662) |
| Completeness (%) | 92.3(94.6) |
| Redundancy | 3.3(3.4) |
| Wilson B-factor | 71.44 |
| Rmerge | 0.086(0.557) |
| I/σI | 16.1(1.9) |
| Refinement | |
| Resolution (Å) | 50~3.00 |
| Rwork | 0.2001 |
| Rfree | 0.2623 |
| No. atoms | 19954 |
| Protein | 19894 |
| ligands | 60 |
| Protein residues | 2533 |
| Ramachandran plot | |
| Favored (%) | 95.0 |
| Allowed (%) | 4.7 |
| Outliers (%) | 0.2 |
| Average B-factors | 75.76 |
| Protein | 75.62 |
| ligands | 119.43 |
| R.m.s. deviations | |
| Bond lengths (Å) | 0.010 |
| Bond angles (°) | 1.42 |
*Values for the highest resolution shell are given in parentheses.