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. 2016 May 20;6(4):187–193. doi: 10.1007/s13659-016-0097-3

Table 2.

13C (150 MHz) NMR data of compounds 16 [δ in ppm, J in Hz]

No. 1 2 3 4 5 6
1 32.7 t 32.5 t 40.6 t 33.7 t 32.0 t 153.5 d
2 30.4 t 30.3 t 32.6 t 37.8 t 30.2 t 127.2 d
3 89.0 d 88.7 d 87.8 d 215.3 s 88.9 d 204.3 s
4 41.7 s 41.3 s 42.7 s 50.4 s 41.3 s 46.6 s
5 47.9 d 47.3 d 51.1 d 48.4 d 47.8 d 47.2 d
6 21.4 t 21.1 t 25.0 t 21.4 t 21.3 t 25.7 t
7 26.7 t 26.3 t 30.6 t 26.1 t 30.3 t 20.3 t
8 49.0 d 47.6 d 50.4 d 46.1 d 47.1 d 45.7 d
9 20.3 s 20.5 s 140.3 s 21.9 s 20.2 s 25.8 s
10 26.9 s 27.0 s 138.7 s 26.6 s 27.4 s 30.6 s
11 26.7 t 37.8 t 135.9 d 41.0 t 26.7 t 46.1 t
12 34.4 t 77.6 d 46.7 s 72.6 d 30.3 t 210.8 s
13 42.2 s 46.3 s 46.7 s 51.5 s 47.5 s 47.5 s
14 47.6 s 48.6 s 49.8 s 48.2 s 49.9 s 60.8 s
15 80.6 d 79.6 d 79.2 d 44.0 t 79.3 d 46.1 t
16 112.3 s 112.6 s 112.7 s 72.8 d 151.3 s 73.0 d
17 59.9 d 59.9 d 58.7 d 53.3 d 121.7 s 48.7 d
18 19.0 q 13.1 q 11.9 q 13.7 q 24.6 q 14.6 q
19 31.2 t 31.2 t 129.6 d 29.6 t 32.4 t 32.6 t
20 24.4 d 24.3 d 24.0 d 35.1 d 27.9 d 25.7 d
21 19.9 q 20.1 q 21.2 q 18.8 q 20.7 q 21.8 q
22 38.5 t 38.8 t 38.9 t 87.9 d 37.2 t 41.3 t
23 72.2 d 74.9 d 72.4 d 106.0 s 77.0 d 106.9 s
24 90.5 d 86.9 d 90.6 d 83.8 d 80.2 d 86.3 d
25 71.3 s 146.1 s 71.4 s 83.9 s 72.3 s 78.2 s
26 24.3 q 113.5 t 27.6 q 25.3 q 27.1 q 78.9 t
27 25.7 q 18.5 q 26.0 q 28.3 q 28.5 q 23.6 q
28 12.2 q 12.4 q 10.4 q 21.1 q 15.6 q 20.3 q
29 26.0 q 25.7 q 25.0 q 22.9 q 25.7 q 22.2 q
30 15.7 q 15.5 q 15.4 q 20.1 q 14.6 q 19.6 q
AcO-12 21.6 q
170.9 s
AcO-24 21.3 q
171.4 s
Sugar
 1′ 107.7 d 105.0 d 108.0 d 105.0 d
 2′ 76.1 d 76.0 d 76.1 d 76.0 d
 3′ 75.3 d 76.6 d 79.2 d 76.6 d
 4′ 73.5 d 71.9 d 71.7 d 71.7 d
 5′ 63.5 t 67.4 t 67.7 t 67.5 t
AcO-2′ 170.4 1 170.4 s
22.0 21.6 q
AcO-4′ 21.2 q
171.0 s