Table 2.
Sample | Degradation | Particle Size | NanoCluster D50 Size | BET Surface Area | DSC Melting Temperature |
---|---|---|---|---|---|
Stock Danazol | - | 2.5 um* | 2.5 um | 3.28±0.03 m2/g | 227.49 ºC |
5 Hour Milled | 0.39±0.20% | 341.2±8.6 nm | 2.0 um | 25.86±0.10 m2/g | 223.82 ºC |
10 Hour Milled | 0.90±0.48% | 354.5±10.0 nm | 1.8 um | 36.75±0.14 m2/g | 222.08 ºC |
15 Hour Milled | 1.23±0.06% | 412.8±11.8 nm | 1.6 um | 47.65±0.26 m2/g | 220.89 ºC |
Nanoparticle Suspension | - | 234.8±1.9 nm | - | 34.07 m2/g** | 224.78 ºC |
Calculated from BET;
Calculated from particle size45
Particle size was determined using DLS while MFI was used to determine NanoCluster D50 size.