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. 2016 Aug 1;24(15):3255–3258. doi: 10.1016/j.bmc.2016.03.030

Table 2.

Analytical data of the synthesized peptides

Peptide Calculated MW Observed MW HPLC gradient (% MeCN in H2O incl. 0.05% TFA) Retention time (min)
1 1355 1378.0 [M+Na]+ 10 → 50 9.8
2 1470 1493.0 [M+Na]+ 10 → 50 13.6
3 1448 1449.0 [M+H]+ 10 → 50 11.2
4 1485 1509.9 [M+Na]+ 10 → 50 8.5
5 1422 1423.2 [M+H]+ 10 → 50 10.5
6 1369 1392.9 [M+Na]+ 10 → 50 3.0
7 1296 1296.3 [M+H]+ 10 → 50 1.8
8 1341 1342.1 [M+H]+ 10 → 50 8.8