Table 2.
Peptide | Calculated MW | Observed MW | HPLC gradient (% MeCN in H2O incl. 0.05% TFA) | Retention time (min) |
---|---|---|---|---|
1 | 1355 | 1378.0 [M+Na]+ | 10 → 50 | 9.8 |
2 | 1470 | 1493.0 [M+Na]+ | 10 → 50 | 13.6 |
3 | 1448 | 1449.0 [M+H]+ | 10 → 50 | 11.2 |
4 | 1485 | 1509.9 [M+Na]+ | 10 → 50 | 8.5 |
5 | 1422 | 1423.2 [M+H]+ | 10 → 50 | 10.5 |
6 | 1369 | 1392.9 [M+Na]+ | 10 → 50 | 3.0 |
7 | 1296 | 1296.3 [M+H]+ | 10 → 50 | 1.8 |
8 | 1341 | 1342.1 [M+H]+ | 10 → 50 | 8.8 |