Table 1.
Product | Yield (%)a | Time (hr) | Mp (°C) |
---|---|---|---|
60 | 8 | 113-115 | |
65 | 6 | 80-81 | |
87 | 6 | 84-86 | |
75 | 3 | 96-97 | |
70 | 3 | 99-101 | |
77 | 3 | 90-91 | |
80 | 3 | 111-113 | |
75 | 3 | 94-96 | |
65 | 16 | 91-92 | |
70 | 12 | 170-171 | |
75 | 24 | 114-115 |
Isolated yields
Product | Yield (%)a | Time (hr) | Mp (°C) |
---|---|---|---|
60 | 8 | 113-115 | |
65 | 6 | 80-81 | |
87 | 6 | 84-86 | |
75 | 3 | 96-97 | |
70 | 3 | 99-101 | |
77 | 3 | 90-91 | |
80 | 3 | 111-113 | |
75 | 3 | 94-96 | |
65 | 16 | 91-92 | |
70 | 12 | 170-171 | |
75 | 24 | 114-115 |
Isolated yields