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. Author manuscript; available in PMC: 2016 Jul 25.
Published in final edited form as: J Med Chem. 2015 Nov 16;58(22):8896–8906. doi: 10.1021/acs.jmedchem.5b01187

Table 1.

Structures, reaction times, yields, and melting points for the synthesis of carbamate and carbonate dimers of melampomagnolide B from intermediate 6

Product Yield (%)a Time (hr) Mp (°C)
graphic file with name nihms-784600-t0004.jpg 60 8 113-115
graphic file with name nihms-784600-t0005.jpg 65 6 80-81
graphic file with name nihms-784600-t0006.jpg 87 6 84-86
graphic file with name nihms-784600-t0007.jpg 75 3 96-97
graphic file with name nihms-784600-t0008.jpg 70 3 99-101
graphic file with name nihms-784600-t0009.jpg 77 3 90-91
graphic file with name nihms-784600-t0010.jpg 80 3 111-113
graphic file with name nihms-784600-t0011.jpg 75 3 94-96
graphic file with name nihms-784600-t0012.jpg 65 16 91-92
graphic file with name nihms-784600-t0013.jpg 70 12 170-171
graphic file with name nihms-784600-t0014.jpg 75 24 114-115
a

Isolated yields