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Autosampler and flow-injection conditions.
|
Autosampler Settings |
|
|---|---|
| Parameter | Setting |
| Syringe Size | 100 μL |
| Filling Speed | 10 μL/s |
| Injection Speed | 10 μL/s |
| Injection Volume | 15 μL |
| Loop Size | 10 μL |
| Loop Method | overfill |
| Wash Solvent | same as mobile phase |
| Wash Cycle | one wash with mobile phase to clean the syringe, then a second wash with mobile phase to clean the syringe and the injection value (total volume ~30-50 μL). |
