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. 2016 Jun 23;138(29):9183–9192. doi: 10.1021/jacs.6b04325

Figure 2.

Figure 2

(a) Time-dependent photocatalytic aldehyde and H2 production with NCNCNx (5 mg), NiP (50 nmol), 4-MBA (30 μmol) in KPi (0.02 M, pH 4.5, 3 mL) under 1 sun irradiation (AM 1.5G) at 25 °C. For each time-point, three vials were irradiated for a specified number of hours and then worked-up. (b) Simultaneous H2 and aldehyde production under optimized reaction conditions in the absence (AM 1.5G) and in the presence of a UV-filter (λ > 400 nm). The pair of hollow and filled symbols of the same shape and color corresponds to H2 and aldehyde production, respectively, under the specified reaction conditions. Control experiments in the absence of NiP, 4-MBA, NCNCNx and in the dark are also shown.