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. 2016 Jun 23;138(29):9183–9192. doi: 10.1021/jacs.6b04325

Figure 4.

Figure 4

Photocatalytic H2 and aldehyde production with NCNCNx or H2NCNx (5 mg), in the presence of 4-MBA (30 μmol) and NiP (50 nmol) in KPi (0.02 M, pH 4.5, 3 mL) were conducted under 1 sun irradiation (100 mW cm–2, AM 1.5G, 25 °C). Photocatalytic experiments in the presence of NCNCNx or H2NCNx (5 mg), 4-MBA (30 μmol), and H2PtCl6 (10 μL, 8 wt %) in KPi (0.02 M, pH 4.5, 3 mL) were also carried out. The pair of hollow and filled symbols of the same shape and color corresponds to H2 and aldehyde production, respectively, under the specified reaction conditions.