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. Author manuscript; available in PMC: 2017 Apr 11.
Published in final edited form as: Angew Chem Int Ed Engl. 2016 Feb 29;55(16):4914–4918. doi: 10.1002/anie.201510570

Table 2.

Substrates with sensitive functionality and/or sp and sp3 carbon-based reaction partners

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Reaction conditions for A and B: 0.5 mmol ArX, 0.53–0.6 mmol Ar’[B], 1000 ppm Pd(OAc)2 0.01 m in toluene, 1020 ppm HandaPhos, 0.75–1.0 mmol Et3N, 1.0 mL 2 wt % Nok in H2O, RT. Unless otherwise mentioned, RT = room temperature For Scheme B, reaction temperature is 45 °C. *Y was added in two portions at 12 h intervals (see SI, pages S17–S18 for a general procedure).