. 2016 Mar 24;7(7):4407–4417. doi: 10.1039/c6sc00197a

Table 2. Preparation of SPIAd ylides and radiofluorination of heterocycles ^a .

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^aRadiochemical conversions by rTLC; identities confirmed by coinjection on radioHPLC; conditions: precursor (3.5 µmol), anhydrous DMF (0.4 mL), TEAB (0.6 mg), [¹⁸F]fluoride (ca. 50 µCi), 120 °C, 10 min.

Table 2. Preparation of SPIAd ylides and radiofluorination of heterocycles a .

Table 2. Preparation of SPIAd ylides and radiofluorination of heterocycles ^a .