Table 4.

Experimental and literature ¹³C chemical shift data for DON in CDCl₃, acetone-d₆, and DMSO-d₆.

13C	CDCl3		Acetone-d6		DMSO-d6
	Lit.a	Exp.	Lit.a	Exp.	Lit.a	Exp.
2	80.6	80.80	81.6	80.84	80.2	80.62
3	68.6	69.17	69.3	68.60	67.8	$68.17$b
4	43.0	43.21	44.4	43.64	43.7	44.12
5	47.2	46.46	46.5	45.79	45.4	45.75
6	52.1	51.96	53.0	52.20	51.8	52.18
7	70.2	70.39	70.6	69.71	69.3	69.61
8	202.3	199.87	200.7	199.83	200.0	200.58
9	135.7	135.96	135.6	134.68	134.8	135.18
10	138.5	138.4	139.7	138.99	138.2	138.71
11	74.4	74.53	75.4	74.57	74.5	74.84
12	65.6	65.61	66.5	65.66	66.0	66.31
13	46.0	47.41	47.5	46.66	46.7	47.11
14	13.9	14.34	14.5	13.71	14.5	14.84
15	61.4	62.56	61.5	60.80	60.1	60.47
16	14.9	15.37	15.2	14.41	15.1	15.46

^aAll literature data obtained from Jarvis et al. (1990).

^bBlue indicates increase and red decrease in chemical shift with respect to CDCl₃. No error estimates available from fitting. The experimental digital resolution is 0.55 Hz or 0.007 ppm.