| Crystal data |
| Chemical formula |
[Co(C11H13O2)2(C6H6N2O)2(H2O)2]·2H2O |
|
M
r
|
729.69 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
296 |
|
a, b, c (Å) |
7.9608 (5), 10.0679 (6), 12.3007 (7) |
| α, β, γ (°) |
72.087 (2), 74.841 (3), 78.660 (3) |
|
V (Å3) |
898.17 (9) |
|
Z
|
1 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.54 |
| Crystal size (mm) |
0.45 × 0.34 × 0.28 |
| |
| Data collection |
| Diffractometer |
Bruker SMART BREEZE CCD |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2012 ▸) |
|
T
min, T
max
|
0.80, 0.86 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
19515, 4491, 4226 |
|
R
int
|
0.024 |
| (sin θ/λ)max (Å−1) |
0.669 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.036, 0.101, 1.04 |
| No. of reflections |
4491 |
| No. of parameters |
276 |
| No. of restraints |
156 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) |
0.57, −0.20 |
