| Bruker Photon-100 CMOS diffractometer | 10345 reflections with I > 2σ(I) |
| Radiation source: sealedtube | Rint = 0.043 |
| φ and ω scans | θmax = 79.0°, θmin = 3.4° |
| Absorption correction: multi-scan (SADABS; Bruker,2014/5) | h = −13→12 |
| Tmin = 0.669, Tmax = 0.754 | k = −13→13 |
| 53613 measured reflections | l = −48→48 |
| 10773 independent reflections |