| Bruker SMART APEXII CCD diffractometer | 2277 reflections with I > 2σ(I) |
| Radiation source: fine-focus sealed tube | Rint = 0.037 |
| ω scans | θmax = 71.1°, θmin = 3.6° |
| Absorption correction: multi-scan (SADABS; Bruker, 2013) | h = −15→15 |
| Tmin = 0.599, Tmax = 0.753 | k = −11→11 |
| 18263 measured reflections | l = −15→16 |
| 2895 independent reflections |
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