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. 2016 Jun 21;72(Pt 7):988–994. doi: 10.1107/S205698901600935X
Si1—O1 1.722 (3) C18—C23 1.402 (5)
Si1—O2 1.739 (3) C19—C20 1.401 (6)
Si1—N3 1.904 (3) C19—H19A 0.9500
Si1—N5 1.915 (3) C20—C21 1.384 (6)
Si1—N7 1.917 (3) C20—H20A 0.9500
Si1—N1 1.918 (3) C21—C22 1.377 (5)
O1—C33 1.379 (4) C21—H21A 0.9500
O2—C40 1.367 (4) C22—C23 1.391 (6)
N1—C1 1.358 (5) C22—H22A 0.9500
N1—C8 1.378 (5) C23—C24 1.435 (5)
N2—C9 1.302 (5) C25—C26 1.453 (5)
N2—C8 1.322 (5) C26—C27 1.386 (6)
N3—C9 1.382 (5) C26—C31 1.389 (5)
N3—C16 1.387 (5) C27—C28 1.384 (5)
N4—C17 1.313 (5) C27—H27A 0.9500
N4—C16 1.320 (5) C28—C29 1.394 (6)
N5—C24 1.383 (5) C28—H28A 0.9500
N5—C17 1.393 (4) C29—C30 1.377 (6)
N6—C25 1.325 (5) C29—H29A 0.9500
N6—C24 1.326 (4) C30—C31 1.391 (5)
N7—C32 1.378 (5) C30—H30A 0.9500
N7—C25 1.385 (5) C31—C32 1.457 (5)
N8—C32 1.318 (5) C33—C34 1.389 (5)
N8—C1 1.329 (5) C33—C38 1.395 (6)
C1—C2 1.464 (5) C34—C35 1.410 (5)
C2—C7 1.386 (5) C34—H34A 0.9500
C2—C3 1.388 (5) C35—C36 1.377 (7)
C3—C4 1.367 (6) C35—C39 1.501 (6)
C3—H3A 0.9500 C36—C37 1.376 (7)
C4—C5 1.418 (6) C36—H36A 0.9500
C4—H4A 0.9500 C37—C38 1.378 (5)
C5—C6 1.377 (5) C37—H37A 0.9500
C5—H5A 0.9500 C38—H38A 0.9500
C6—C7 1.395 (5) C39—H39A 0.9800
C6—H6A 0.9500 C39—H39B 0.9800
C7—C8 1.459 (5) C39—H39C 0.9800
C9—C10 1.451 (5) C40—C41 1.391 (5)
C10—C15 1.395 (6) C40—C45 1.400 (6)
C10—C11 1.402 (6) C41—C42 1.381 (5)
C11—C12 1.374 (5) C41—H41A 0.9500
C11—H11A 0.9500 C42—C43 1.399 (7)
C12—C13 1.398 (6) C42—C46 1.503 (6)
C12—H12A 0.9500 C43—C44 1.390 (6)
C13—C14 1.390 (6) C43—H43A 0.9500
C13—H13A 0.9500 C44—C45 1.374 (5)
C14—C15 1.385 (5) C44—H44A 0.9500
C14—H14A 0.9500 C45—H45A 0.9500
C15—C16 1.437 (5) C46—H46A 0.9800
C17—C18 1.444 (6) C46—H46B 0.9800
C18—C19 1.387 (5) C46—H46C 0.9800
O1—Si1—O2 179.59 (14) C20—C19—H19A 121.7
O1—Si1—N3 92.10 (13) C21—C20—C19 121.3 (3)
O2—Si1—N3 88.17 (13) C21—C20—H20A 119.4
O1—Si1—N5 91.88 (14) C19—C20—H20A 119.4
O2—Si1—N5 88.43 (13) C22—C21—C20 122.2 (4)
N3—Si1—N5 89.72 (13) C22—C21—H21A 118.9
O1—Si1—N7 87.84 (13) C20—C21—H21A 118.9
O2—Si1—N7 91.89 (13) C21—C22—C23 117.4 (4)
N3—Si1—N7 179.9 (2) C21—C22—H22A 121.3
N5—Si1—N7 90.18 (13) C23—C22—H22A 121.3
O1—Si1—N1 87.88 (13) C22—C23—C18 120.7 (3)
O2—Si1—N1 91.81 (14) C22—C23—C24 132.5 (3)
N3—Si1—N1 90.80 (13) C18—C23—C24 106.6 (3)
N5—Si1—N1 179.44 (19) N6—C24—N5 127.2 (3)
N7—Si1—N1 89.30 (13) N6—C24—C23 122.2 (3)
C33—O1—Si1 128.6 (2) N5—C24—C23 110.6 (3)
C40—O2—Si1 128.2 (2) N6—C25—N7 127.7 (3)
C1—N1—C8 107.7 (3) N6—C25—C26 122.0 (3)
C1—N1—Si1 127.1 (3) N7—C25—C26 110.2 (3)
C8—N1—Si1 125.2 (2) C27—C26—C31 121.9 (3)
C9—N2—C8 121.4 (3) C27—C26—C25 131.9 (3)
C9—N3—C16 106.6 (3) C31—C26—C25 106.2 (3)
C9—N3—Si1 125.9 (2) C28—C27—C26 116.8 (4)
C16—N3—Si1 127.1 (3) C28—C27—H27A 121.6
C17—N4—C16 122.0 (3) C26—C27—H27A 121.6
C24—N5—C17 106.3 (3) C27—C28—C29 121.3 (4)
C24—N5—Si1 126.8 (2) C27—C28—H28A 119.3
C17—N5—Si1 126.8 (3) C29—C28—H28A 119.3
C25—N6—C24 121.7 (3) C30—C29—C28 121.9 (3)
C32—N7—C25 106.9 (3) C30—C29—H29A 119.1
C32—N7—Si1 126.5 (3) C28—C29—H29A 119.1
C25—N7—Si1 126.3 (2) C29—C30—C31 116.9 (4)
C32—N8—C1 119.9 (3) C29—C30—H30A 121.5
N8—C1—N1 128.5 (4) C31—C30—H30A 121.5
N8—C1—C2 121.4 (3) C26—C31—C30 121.1 (3)
N1—C1—C2 110.1 (3) C26—C31—C32 107.0 (3)
C7—C2—C3 121.9 (4) C30—C31—C32 131.8 (4)
C7—C2—C1 106.1 (3) N8—C32—N7 128.4 (3)
C3—C2—C1 131.9 (3) N8—C32—C31 121.9 (3)
C4—C3—C2 117.4 (3) N7—C32—C31 109.7 (3)
C4—C3—H3A 121.3 O1—C33—C34 120.0 (4)
C2—C3—H3A 121.3 O1—C33—C38 120.4 (3)
C3—C4—C5 121.2 (3) C34—C33—C38 119.5 (3)
C3—C4—H4A 119.4 C33—C34—C35 121.0 (4)
C5—C4—H4A 119.4 C33—C34—H34A 119.5
C6—C5—C4 121.1 (4) C35—C34—H34A 119.5
C6—C5—H5A 119.5 C36—C35—C34 118.5 (4)
C4—C5—H5A 119.5 C36—C35—C39 121.3 (4)
C5—C6—C7 117.4 (3) C34—C35—C39 120.1 (4)
C5—C6—H6A 121.3 C37—C36—C35 120.1 (4)
C7—C6—H6A 121.3 C37—C36—H36A 120.0
C2—C7—C6 120.9 (3) C35—C36—H36A 120.0
C2—C7—C8 106.6 (3) C36—C37—C38 122.3 (4)
C6—C7—C8 132.4 (3) C36—C37—H37A 118.8
N2—C8—N1 128.4 (3) C38—C37—H37A 118.8
N2—C8—C7 122.2 (3) C37—C38—C33 118.6 (4)
N1—C8—C7 109.4 (3) C37—C38—H38A 120.7
N2—C9—N3 128.3 (3) C33—C38—H38A 120.7
N2—C9—C10 122.0 (4) C35—C39—H39A 109.5
N3—C9—C10 109.7 (3) C35—C39—H39B 109.5
C15—C10—C11 120.6 (3) H39A—C39—H39B 109.5
C15—C10—C9 106.8 (3) C35—C39—H39C 109.5
C11—C10—C9 132.6 (3) H39A—C39—H39C 109.5
C12—C11—C10 117.4 (4) H39B—C39—H39C 109.5
C12—C11—H11A 121.3 O2—C40—C41 120.7 (4)
C10—C11—H11A 121.3 O2—C40—C45 120.1 (3)
C11—C12—C13 122.0 (4) C41—C40—C45 119.2 (3)
C11—C12—H12A 119.0 C42—C41—C40 121.7 (4)
C13—C12—H12A 119.0 C42—C41—H41A 119.2
C14—C13—C12 120.7 (3) C40—C41—H41A 119.2
C14—C13—H13A 119.6 C41—C42—C43 118.5 (4)
C12—C13—H13A 119.6 C41—C42—C46 122.0 (4)
C15—C14—C13 117.6 (4) C43—C42—C46 119.5 (4)
C15—C14—H14A 121.2 C44—C43—C42 119.9 (3)
C13—C14—H14A 121.2 C44—C43—H43A 120.0
C14—C15—C10 121.6 (4) C42—C43—H43A 120.0
C14—C15—C16 131.9 (4) C45—C44—C43 121.3 (4)
C10—C15—C16 106.4 (3) C45—C44—H44A 119.4
N4—C16—N3 127.1 (3) C43—C44—H44A 119.4
N4—C16—C15 122.5 (3) C44—C45—C40 119.2 (4)
N3—C16—C15 110.4 (3) C44—C45—H45A 120.4
N4—C17—N5 127.0 (4) C40—C45—H45A 120.4
N4—C17—C18 123.0 (3) C42—C46—H46A 109.5
N5—C17—C18 110.0 (3) C42—C46—H46B 109.5
C19—C18—C23 121.8 (4) H46A—C46—H46B 109.5
C19—C18—C17 131.7 (4) C42—C46—H46C 109.5
C23—C18—C17 106.4 (3) H46A—C46—H46C 109.5
C18—C19—C20 116.6 (4) H46B—C46—H46C 109.5
C18—C19—H19A 121.7