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. 2016 Jun 21;72(Pt 7):988–994. doi: 10.1107/S205698901600935X
Bruker Kappa APEX DUO CCD diffractometer 4085 independent reflections
Radiation source: fine-focus sealed tube 2969 reflections with I > 2σ(I)
Multi-layer optics monochromator Rint = 0.104
φ and ω scans θmax = 66.8°, θmin = 3.4°
Absorption correction: multi-scan (TWINABS; Bruker, 2007) h = −12→12
Tmin = 0.621, Tmax = 0.753 k = −30→30
120855 measured reflections l = −38→38