Bruker Kappa APEX DUO CCD diffractometer | 4085 independent reflections |
Radiation source: fine-focus sealed tube | 2969 reflections with I > 2σ(I) |
Multi-layer optics monochromator | Rint = 0.104 |
φ and ω scans | θmax = 66.8°, θmin = 3.4° |
Absorption correction: multi-scan (TWINABS; Bruker, 2007) | h = −12→12 |
Tmin = 0.621, Tmax = 0.753 | k = −30→30 |
120855 measured reflections | l = −38→38 |