Crystal structures of bis­(phen­oxy)silicon phthalocyanines: increasing π–π inter­actions, solubility and disorder and no halogen bonding observed

. 2016 Jun 21;72(Pt 7):988–994. doi: 10.1107/S205698901600935X

	U¹¹	U²²	U³³	U¹²	U¹³	U²³
Si1	0.0459 (6)	0.0491 (6)	0.0323 (5)	0.0052 (4)	0.000	0.000
O1	0.0573 (12)	0.0531 (11)	0.0402 (11)	−0.0034 (9)	−0.0045 (8)	0.0066 (8)
N1	0.0552 (19)	0.0534 (18)	0.0344 (16)	0.0052 (14)	0.000	0.000
N2	0.0658 (15)	0.0622 (14)	0.0390 (13)	0.0115 (12)	0.0092 (11)	0.0023 (11)
N3	0.0516 (13)	0.0526 (13)	0.0366 (12)	0.0080 (10)	0.0062 (10)	0.0035 (9)
N4	0.0455 (12)	0.0558 (13)	0.0387 (12)	0.0043 (10)	0.0028 (10)	0.0038 (9)
N5	0.0434 (16)	0.0514 (17)	0.0295 (15)	0.0019 (13)	0.000	0.000
C1	0.066 (2)	0.097 (2)	0.0342 (15)	0.0023 (16)	0.0047 (14)	−0.0033 (15)
C2	0.0594 (18)	0.080 (2)	0.0410 (16)	0.0041 (15)	0.0065 (14)	−0.0070 (14)
C3	0.0555 (16)	0.0632 (17)	0.0395 (15)	−0.0014 (13)	−0.0014 (13)	−0.0007 (12)
C4	0.0522 (15)	0.0568 (16)	0.0363 (14)	0.0049 (13)	0.0058 (12)	−0.0003 (11)
C5	0.0628 (18)	0.0565 (16)	0.0411 (16)	0.0103 (14)	0.0108 (13)	0.0017 (12)
C6	0.0665 (19)	0.0603 (17)	0.0490 (17)	0.0188 (14)	0.0146 (14)	0.0095 (13)
C7	0.091 (3)	0.077 (2)	0.059 (2)	0.032 (2)	0.0247 (18)	0.0101 (17)
C8	0.088 (3)	0.080 (2)	0.086 (3)	0.039 (2)	0.024 (2)	0.016 (2)
C9	0.075 (2)	0.080 (2)	0.084 (3)	0.034 (2)	0.007 (2)	0.0160 (19)
C10	0.0606 (18)	0.0678 (19)	0.0586 (18)	0.0153 (15)	0.0047 (15)	0.0135 (15)
C11	0.0535 (16)	0.0553 (16)	0.0518 (18)	0.0100 (13)	0.0095 (13)	0.0102 (13)
C12	0.0447 (14)	0.0535 (15)	0.0437 (15)	0.0061 (12)	0.0029 (12)	0.0086 (12)
C13	0.0395 (13)	0.0524 (14)	0.0379 (14)	−0.0013 (11)	−0.0006 (11)	0.0006 (11)
C14	0.0406 (13)	0.0557 (15)	0.0379 (14)	−0.0030 (11)	0.0018 (11)	0.0012 (11)
C15	0.0486 (15)	0.0730 (19)	0.0403 (15)	0.0000 (13)	−0.0051 (13)	0.0035 (13)
C16	0.0605 (18)	0.082 (2)	0.0365 (14)	−0.0010 (15)	−0.0072 (14)	0.0028 (14)
C17	0.0517 (16)	0.0635 (18)	0.0530 (17)	−0.0010 (13)	0.0000 (14)	0.0167 (14)
C18	0.0513 (17)	0.098 (2)	0.0487 (18)	−0.0062 (16)	−0.0014 (14)	0.0108 (17)
C19	0.072 (2)	0.159 (5)	0.068 (3)	−0.022 (3)	0.008 (2)	0.037 (3)
C20	0.117 (4)	0.122 (4)	0.129 (4)	−0.012 (3)	0.013 (3)	0.076 (4)
C21	0.127 (4)	0.085 (3)	0.164 (5)	0.008 (3)	0.054 (4)	0.058 (3)
C22	0.092 (3)	0.059 (2)	0.120 (3)	0.000 (2)	0.033 (2)	0.022 (2)
C23	0.155 (5)	0.059 (2)	0.171 (5)	−0.016 (3)	0.082 (4)	−0.007 (3)
C24	0.259 (8)	0.144 (5)	0.135 (5)	−0.085 (6)	0.066 (5)	−0.030 (4)
C25	0.143 (5)	0.085 (3)	0.316 (9)	−0.011 (4)	0.099 (6)	−0.056 (5)
C26	0.183 (7)	0.172 (7)	0.324 (11)	0.024 (6)	0.067 (8)	−0.090 (8)