Stoe StadiVari with pixel array detector diffractometer | 3016 independent reflections |
Radiation source: IµS microfocus source | 2046 reflections with I > 2σ(I) |
Plane graphite monochromator | Rint = 0.102 |
φ and ω scans | θmax = 29.6°, θmin = 2.8° |
Absorption correction: multi-scan (X-AREA and X-RED; Stoe, 2013) | h = −17→20 |
Tmin = 0.366, Tmax = 0.921 | k = −12→20 |
34206 measured reflections | l = −27→27 |