Table 3. Cross-Coupling of Aryl Tosylates with Alkylbis(catecholato)silicates in Photoredox/Ni Cross-Couplinga.
R′ = R″ = Et or R′ = H, R″ = i-Pr.
Conversion determined by HPLC.
Inseparable cyclohexyl dimer impurity present in 1H and 13C NMRs
R′ = R″ = Et or R′ = H, R″ = i-Pr.
Conversion determined by HPLC.
Inseparable cyclohexyl dimer impurity present in 1H and 13C NMRs