Table 4. Unsuccessful Cross-Coupling Partners in Photoredox/Ni Cross-Couplinga.
Reacted using 2 mol % [Ru(bpy)3](PF6), 10 mol % [NiCl2(dme)] and 10 mol % dttbpy in DMF (0.1 M).
Reacted with 2a.
Reacted with 2c.
Reacted with silicate 1a.
Reacted using 2 mol % [Ru(bpy)3](PF6), 10 mol % [NiCl2(dme)] and 10 mol % dttbpy in DMF (0.1 M).
Reacted with 2a.
Reacted with 2c.
Reacted with silicate 1a.