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. 2016 Jul 27;12(3):1873–1878. doi: 10.3892/etm.2016.3556

Table I.

13C-NMR spectra data of compounds 1–8 (δ, ppm; compounds 4 and 8 were detected at 75 MHz, others at 125 MHz; compounds 1, 2, 3, 4, 6 and 7 dissolved in CD3OD, compound 5 dissolved in DMSO, and compound 8 dissolved in acetone-d6; OMe, OCH3).

Compound no. 1 2 3 4 5 6 7 8
  2 166.24 148.15 160.89 147.99 164.17 164.46 164.73 158.15
  3 103.80 137.17 104.15 137.24 103.04 102.46 104.62 135.63
  4 184.23 177.44 183.79 177.34 181.77 184.31 183.66 179.18
  5 154.70 158.35 163.13 158.23 157.48 152.69 162.33 163.06
  6 132.97 99.38 123.75 99.22 98.90 131.70 99.78 99.35
  7 158.90 165.77 166.09 162.52 163.88 157.66 165.61 164.77
  8   95.38   94.55   95.31   94.39   94.16   94.17   94.75   94.35
  9 154.70 162.53 156.19 165.58 161.22 152.69 158.25 157.63
10 105.78 104.56 105.39 104.52 103.77 104.87 103.89 105.75
  1′ 123.78 123.81 124.69 148.77 121.38 122.14 122.31 122.43
  2′ 110.75 130.69 110.70 115.98 128.56 128.45 114.22 115.99
  3′ 149.52 116.35 149.58 124.14 116.05 116.15 146.78 145.68
  4′ 152.13 160.57 152.52 146.22 161.06 161.32 150.71 148.85
  5′ 116.81 116.35 116.86 116.22 116.05 116.15 116.01 116.56
  6′ 121.76 130.69 121.77 121.67 128.56 128.45 120.46 122.73
  OMe 56.71 56.72 59.85
  OMe 60.94
  1′′ 102.57
  2′′ 71.26)
  3′′ 71.97)
  4′′ 72.86)
  5′′ 71.19
  6′′ 17.63

The table values represent 13C-NMR spectra data of compounds 1–8. OMe represents OCH3. NMR, nuclear magnetic resonance; DMSO, dimethyl sulfoxide.