Table I.
Compound no. | 1 | 2 | 3 | 4 | 5 | 6 | 7 | 8 |
---|---|---|---|---|---|---|---|---|
2 | 166.24 | 148.15 | 160.89 | 147.99 | 164.17 | 164.46 | 164.73 | 158.15 |
3 | 103.80 | 137.17 | 104.15 | 137.24 | 103.04 | 102.46 | 104.62 | 135.63 |
4 | 184.23 | 177.44 | 183.79 | 177.34 | 181.77 | 184.31 | 183.66 | 179.18 |
5 | 154.70 | 158.35 | 163.13 | 158.23 | 157.48 | 152.69 | 162.33 | 163.06 |
6 | 132.97 | 99.38 | 123.75 | 99.22 | 98.90 | 131.70 | 99.78 | 99.35 |
7 | 158.90 | 165.77 | 166.09 | 162.52 | 163.88 | 157.66 | 165.61 | 164.77 |
8 | 95.38 | 94.55 | 95.31 | 94.39 | 94.16 | 94.17 | 94.75 | 94.35 |
9 | 154.70 | 162.53 | 156.19 | 165.58 | 161.22 | 152.69 | 158.25 | 157.63 |
10 | 105.78 | 104.56 | 105.39 | 104.52 | 103.77 | 104.87 | 103.89 | 105.75 |
1′ | 123.78 | 123.81 | 124.69 | 148.77 | 121.38 | 122.14 | 122.31 | 122.43 |
2′ | 110.75 | 130.69 | 110.70 | 115.98 | 128.56 | 128.45 | 114.22 | 115.99 |
3′ | 149.52 | 116.35 | 149.58 | 124.14 | 116.05 | 116.15 | 146.78 | 145.68 |
4′ | 152.13 | 160.57 | 152.52 | 146.22 | 161.06 | 161.32 | 150.71 | 148.85 |
5′ | 116.81 | 116.35 | 116.86 | 116.22 | 116.05 | 116.15 | 116.01 | 116.56 |
6′ | 121.76 | 130.69 | 121.77 | 121.67 | 128.56 | 128.45 | 120.46 | 122.73 |
OMe | 56.71 | 56.72 | 59.85 | |||||
OMe | 60.94 | |||||||
1′′ | 102.57 | |||||||
2′′ | 71.26) | |||||||
3′′ | 71.97) | |||||||
4′′ | 72.86) | |||||||
5′′ | 71.19 | |||||||
6′′ | 17.63 |
The table values represent 13C-NMR spectra data of compounds 1–8. OMe represents OCH3. NMR, nuclear magnetic resonance; DMSO, dimethyl sulfoxide.