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. 2016 Oct 4;121:158–168. doi: 10.1016/j.ejmech.2016.05.043

Scheme 1.

Scheme 1

Reaction Conditions: a) acetic anhydride; b) acetonitrile: water (1:1), aniline, dodecyl hydrogen sulfate sodium salt, rt; c) trifluoroacetic anhydride, TEA, THF; d) aniline, THF, rt.